HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzene-1,2-diamine → HCID 23146400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzene-1,2-diamine | HCID 2782835 | — |
| Reactant | 1-Boc-2-Piperidineacetic Acid | HCID 5058536 | — |
| Product | HCID 23146400 | HCID 23146400 | 61.6% |
Reaction Steps
(RS)-2-Carboxymethyl-piperidine-1-carboxylic acid tert-butyl ester (1.93 g) was heated with 1,2-diamino-3-fluorobenzene (1.00 g) (Kirk, K. L, J. Org. Chem., 1969, 34, 384) as described in Description 18 to afford the title compound (1.14 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893090B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-ba31216588d04487b081d826bf493349 |
| Source note | uspto-grants-2011_02 |