HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 59619400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | 2-Oxa-6-azaspiro[3.3]heptane | HCID 23111887 | — |
| Reactant | HCID 72340489 | HCID 72340489 | — |
| Product | HCID 59619400 | HCID 59619400 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 80, from Rac-(1S,3S)-3-(2-chloro-4-fluoro-benzenesulfonyl)-cyclopentanecarboxylic acid (1-cyano-cyclopropyl)-amide and 2-oxa-6-aza-spiro[3.3]heptane as oxalic acid salt (CAS [1045709-32-7]; Angew. Chem. Int. Ed. 2008, 47, 4512-4515) to afford the desired product as a light yellow oil. MS (EI): 450.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893099B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-4879e4ccf525417a8731f3b1ffb87314 |
| Source note | uspto-grants-2011_02 |