4-Fluoro-2-(trifluoromethyl)benzenesulfonyl Chloride → 4-Fluoro-2-trifluoromethylbenzenethiol

HRID 1367515Notes

Reaction equation

HRID 1367515 reaction equation
BrC1C=CC(S)=C(C(F)(F)F)C=1.[F:13][C:14]1[CH:19]=[CH:18][C:17]([S:20](Cl)(=O)=O)=[C:16]([C:24]([F:27])([F:26])[F:25])[CH:15]=1>>[F:13][C:14]1[CH:19]=[CH:18][C:17]([SH:20])=[C:16]([C:24]([F:27])([F:25])[F:26])[CH:15]=1

Participants

3

Reactant 2

HCID 27375484-Fluoro-2-(trifluoromethyl)benzenesulfonyl ChlorideHCID 509979974-Bromo-2-(trifluoromethyl)benzenethiol

Product 1

HCID 509980024-Fluoro-2-trifluoromethylbenzenethiol

Procedure

The title compound was prepared in analogy to Example 58, Intermediate 1, using 4-fluoro-2-trifluoromethyl-benzene sulfonyl chloride. Colorless liquid. MS (EI): 195.1 (M−H)−.

Sources & evidence

ORD record
ord-46d88f7dc03441d7a98bbc0efbf36267
Source dataset
uspto-grants-2011_02
Patent number
US07893099B2

Reaction notes

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