HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-fluorothiophenol → HCID 66918678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-fluorothiophenol | HCID 519446 | — |
| Reactant | (1R,2R,4R)-2-(3,3-Difluoro-pyrrolidine-1-carbonyl)-4-methanesulfonyloxy-cyclopentanecarboxylic acid ethyl ester | HCID 86649034 | — |
| Product | HCID 66918678 | HCID 66918678 | — |
Reaction Steps
The title compound was prepared in analogy to example 68/69 step 8 using (1R,2R,4R)-2-(3,3-Difluoro-pyrrolidine-1-carbonyl)-4-methanesulfonyloxy-cyclopentanecarboxylic acid ethyl ester (example 186 step 3) and 2-chloro-4-fluorothiophenol. Light yellow oil (88%). MS (EI): 436.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893099B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-10613c6b5ef84b298702d34ea0cc94f9 |
| Source note | uspto-grants-2011_02 |