HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1R,2R,4R)-2-(3,3-Difluoro-pyrrolidine-1-carbonyl)-4-methanesulfonyloxy-cyclopentanecarboxylic acid ethyl ester → HCID 66919022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1R,2R,4R)-2-(3,3-Difluoro-pyrrolidine-1-carbonyl)-4-methanesulfonyloxy-cyclopentanecarboxylic acid ethyl ester | HCID 86649034 | — |
| Reactant | HCID 178418616 | HCID 178418616 | — |
| Product | HCID 66919022 | HCID 66919022 | — |
Reaction Steps
The title compound was prepared in analogy to example 68/69 step 8 using (1R,2R,4R)-2-(3,3-Difluoro-pyrrolidine-1-carbonyl)-4-methanesulfonyloxy-cyclopentanecarboxylic acid ethyl ester (example 186 step 3) and 2-mercaptopyridine. Light brown semi-solid (74%). MS (EI): 385.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893099B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-06ea5ac083904b32b48460d91733653c |
| Source note | uspto-grants-2011_02 |