HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 58938502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Methyl-4H-pyrido[4,3-d][1,3]oxazin-4-one | HCID 23151370 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 58938502 | HCID 58938502 | — |
Reaction Steps
Compound 17 (350 mg, 21.6 mmol) was mixed with aniline (200 mg, 21.6 mmol) in 3 mL of pyridine. The resulted solution was heated in a microwave for 25 min keeping temperature constant at 250° C. The crude material 18 was concentrated in vacuo, co-evaporated with toluene (3×10 mL), dried under vacuum for 1 h and used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893260B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-38f7768d7c754c81a9f32c70d9c61f9b |
| Source note | uspto-grants-2011_02 |