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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1367832Generated: November 1, 2026

4-Toluenesulfonyl chloride → HCID 66962557, compound

https://huagongshe.com/reaction/1367832

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Toluenesulfonyl chlorideHCID 7397—
ReactantTrimethyl phosphiteHCID 8472—
ReactantHCID 18737468HCID 18737468—
ProductHCID 66962557HCID 66962557—

Reaction Steps

Bis(4-formylphenyl)phenylamine was reduced in ethanol with 2 equivalents of sodium borohydride to obtain bis(4-hydroxymethylphenyl)phenylamine. The obtained bis(4-hydroxymethylphenyl)phenylamine was reacted with equimolar p-toluenesulfonylchloride to replace a hydroxyl group at one end with a toluenesulfonyl group, and then the resultant compound was reacted with trimethylphosphite to yield a triphenylamine phosphate derivative having the structure represented by the Formula (6), as an intermediate compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07894118B2
Source datasetuspto-grants-2011_02
ORD IDord-57f9d6b5fa184b68af31e34888b1d791
Source noteuspto-grants-2011_02