HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 66962557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | HCID 18737468 | HCID 18737468 | — |
| Product | HCID 66962557 | HCID 66962557 | — |
Reaction Steps
Bis(4-formylphenyl)phenylamine was reduced in ethanol with 2 equivalents of sodium borohydride to obtain bis(4-hydroxymethylphenyl)phenylamine. The obtained bis(4-hydroxymethylphenyl)phenylamine was reacted with equimolar p-toluenesulfonylchloride to replace a hydroxyl group at one end with a toluenesulfonyl group, and then the resultant compound was reacted with trimethylphosphite to yield a triphenylamine phosphate derivative having the structure represented by the Formula (6), as an intermediate compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07894118B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-57f9d6b5fa184b68af31e34888b1d791 |
| Source note | uspto-grants-2011_02 |