HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15490947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(2-Bromoethoxy)Benzaldehyde | HCID 262706 | — |
| Reactant | 2,6-Dimethyl-1H-pyrimidin-4-one | HCID 135408640 | — |
| Product | HCID 15490947 | HCID 15490947 | 30% |
Reaction Steps
The title compound (0.8 g, 30%) was prepared from 2,4-dimethyl-1,6-dihydro-6-pyrimidone (1.3 g 10.48 mmol) and 4-[2-bromoethoxy]benzaldehyde (2.4 g, 10.48 mmol) in the presence of a base K2CO3 (2.89 g, 20.96 mmol) by a similar procedure as described in preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573268B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-197f722618394921a00c85a65bb42059 |
| Source note | uspto-grants-2003_06 |