HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → methyl (4E)-2-acetyl-5-phenyl-4-pentenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Cinnamyl bromide | HCID 5357478 | — |
| Reactant | sodium (2E)-4-methoxy4-oxo-2-buten-2-olate | HCID 23681258 | — |
| Product | methyl (4E)-2-acetyl-5-phenyl-4-pentenoate | HCID 11020753 | — |
Reaction Steps
Analogously to Example 28A, 10 g (72.4 mmol) of sodium (2E)-4-methoxy-4-oxo-2-buten-2-olate and 0.40 g (2.41 mmol) of potassium iodide are reacted with 14.3 g (72.4 mmol) of [(1E)-3-bromo-1-propenyl]benzene to give methyl (4E)-2-acetyl-5-phenyl-4-pentenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573263B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-bbee9c6118c04db7923aaaa574d1a179 |
| Source note | uspto-grants-2003_06 |