HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 2-(3,4-dimethoxybenzyl)-5-ethyl-7-[1-(1-hydroxyethyl)-4-phenylbutyl]imidazo[5,1-f][1,2,4]triazin-4(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 7-(1-acetyl-4-phenylbutyl)-2-(3,4-dimethoxybenzyl)-5-ethylimidazo[5,1-f][1,2,4]triazin-4(3H)-one | HCID 135547913 | — |
| Product | 2-(3,4-dimethoxybenzyl)-5-ethyl-7-[1-(1-hydroxyethyl)-4-phenylbutyl]imidazo[5,1-f][1,2,4]triazin-4(3H)-one | HCID 135824729 | — |
Reaction Steps
50 mg (0.10 mmol) of 7-(1-acetyl-4-phenylbutyl)-2-(3,4-dimethoxybenzyl)-5-ethyl-imidazo[5,1-f][1,2,4]triazin-4(3H)-one, analogously to Example 12 are reacted with 19 mg (0.50 mmol) of sodium borohydride to give 2-(3,4-dimethoxybenzyl)-5-ethyl-7-[1-(1-hydroxyethyl)-4-phenylbutyl]imidazo[5,1-f][1,2,4]triazin-4(3H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573263B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-16e0cb05fb434e7da97f60c28b66fd58 |
| Source note | uspto-grants-2003_06 |