HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9894515, compound → HCID 18520283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9894515 | HCID 9894515 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18520283 | HCID 18520283 | — |
Reaction Steps
4N Hydrochloric acid/ethyl acetate solution (1.2 ml) was added to a solution containing N-(3-morpholinopropyl)-3-[2-(octadecyloxy)phenyl]propanamide (1.88 g) in ethyl acetate (38 ml) at room temperature. After being stirred for 45 minutes, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (1.89 g) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573297B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-328c9ff2130d4044b243fa3ca2443740 |
| Source note | uspto-grants-2003_06 |