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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1368376Generated: October 31, 2026

HCID 9894515, compound → HCID 18520283, compound

https://huagongshe.com/reaction/1368376

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9894515HCID 9894515—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
SolventEthyl AcetateHCID 8857—
ProductHCID 18520283HCID 18520283—

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.2 ml) was added to a solution containing N-(3-morpholinopropyl)-3-[2-(octadecyloxy)phenyl]propanamide (1.88 g) in ethyl acetate (38 ml) at room temperature. After being stirred for 45 minutes, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (1.89 g) as white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06573297B2
Source datasetuspto-grants-2003_06
ORD IDord-328c9ff2130d4044b243fa3ca2443740
Source noteuspto-grants-2003_06