HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 67281560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 4-Methyl-5-methylaminosulfonyl-2-oxindole | HCID 69052589 | — |
| Reactant | HCID 85786887 | HCID 85786887 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67281560 | HCID 67281560 | 52% |
Reaction Steps
4-Methyl-5-methylaminosulfonyl-2-oxindole (50 mg, 0.21 mmol) was condensed with [(5-formyl-4-methyl-1H-pyrrole-3-carbonyl)-amino]-acetic acid ethyl ester (100 mg, 0.42 mmol) and piperidine (0.1 mL) in ethanol (2 mL) to give 50 mg (52%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573293B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-ba301a698d7245539bc5ccd3b04e1c15 |
| Source note | uspto-grants-2003_06 |