HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 3-Hydroxy-1,3-diphenylpropan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 18520757 | HCID 18520757 | — |
| Solvent | HCID 86758999 | HCID 86758999 | — |
| Product | 3-Hydroxy-1,3-diphenylpropan-1-one | HCID 10059587 | — |
Reaction Steps
A mixture of phenyl trimethoxy ethylene (0.005 mol) and benzaldehyde (0.005 mol) in ZnCl2-Choline chloride (2:1) melt (0.5 ml) was stirred mechanically for 10 minutes and silylated intermediate was pipetted out and treated with HCl(1N)/MeOH (1:10) to give pure 3-hydroxy 1,3-diphenyl-1-propanone quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06573405B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-8f51075938584ebc9a4fb32c724ffc5f |
| Source note | uspto-grants-2003_06 |