HCID 18518365, compound → HCID 18518373, compound

HRID 1369219Notes

Reaction equation

HRID 1369219 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([CH2:7][CH2:8][C:9]2([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[CH3:19])O)=[CH:5][CH:4]=1.COC1C=C2C(CCC2(C2C=CC=CC=2)O)=CC=1>>[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([CH:7]=[CH:8][CH:9]2[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[CH3:19])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 18518365HCID 18518365, compoundHCID 18518366HCID 18518366, compound

Product 1

HCID 18518373HCID 18518373, compound

Procedure

According to the procedure of Preparation 10 (a), except substituting 6-methoxy-1-(2-methylphenyl)-1-indanol for the 6-methoxy-1-phenyl-1-indanol, the title compound was obtained as a colorless oil following silica gel chromatography (3% EtOAc/hexanes): MS (ES) m/e 237.2 (M+H)+.

Sources & evidence

ORD record
ord-1688266b492446c3b2864cafdf63b36a
Source dataset
uspto-grants-2003_06
Patent number
US06576643B2

Reaction notes

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