HCID 12743485, compound → HCID 18518281, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([OH:12])=[O:11])=[C:5]([C:13](=O)[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[CH3:20])[CH:4]=1.C(C1C=C(OC)C=CC=1CC(O)=O)(=O)C1C=CC=CC=1>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([OH:12])=[O:11])=[C:5]([CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[CH3:20])[CH:4]=1Participants
3
Procedure
According to the procedure of Preparation 10 (c), except substituting 4-methoxy-2-(2-methylbenzoyl)phenylacetic acid for the 2-benzoyl-4-methoxyphenylacetic acid, the title compound was obtained as a viscous oil: MS (ES) m/e 288.2 (M+NH4)+.
Sources & evidence
- ORD record
- ord-ae110780b2cf474eae2d025cd65fe609
- Source dataset
- uspto-grants-2003_06
- Patent number
- US06576643B2
Reaction notes
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