Hydrochloric Acid → HCID 70024995, compound

Participants

Reaction Steps

To 2-acetyl-7,8-dihydro-6H-5-oxa-9-thia-benzocycloheptene-4-carboxylic acid amide (0.40 g, 1.59 mmol) suspended in EtOH (10 mL) was added NaBH4 (0.060 g, 1.59 mmol). The mixture was stirred for 5 min. made acidic with 1 N HCl, and the EtOH removed in vacuuo. The aqueous was extracted with EtOAc. The combined extracts were washed with water, dried over magnesium sulfate and concentrated to a foam (0.35 g, 87%). MS [M+H]+ 252.

Provenance & Evidence