1,6-Hexanediol → HCID 135967528, compound

HRID 1369325Notes

Reaction equation

[OH:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[C:17](=[S:30])[C:18]1[CH:23]=[CH:22][C:21]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:20][CH:19]=1)[O:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12].[CH2:31]([OH:38])[CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][OH:37]>>[OH:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[C:17](=[S:30])[C:18]1[CH:19]=[CH:20][C:21]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:22][CH:23]=1)[O:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][C:31]([O:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:11](=[O:13])[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][O:5][C:4]1[CH:14]=[CH:15][C:16]([C:17](=[S:30])[C:18]2[CH:19]=[CH:20][C:21]([C:24]3[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=3)=[CH:22][CH:23]=2)=[C:2]([OH:1])[CH:3]=1)=[O:38]

Participants

Reactant 2

HCID 123741,6-Hexanediol

HCID 136045367HCID 136045367, compound

Product 1

HCID 135967528HCID 135967528, compound

Procedure

Following the general procedure of Example 13 or Example 17, the title compound is prepared by reacting an equivalent amount of the acid compound of Example 16 with a half equivalent amount of 1,6-hexanediol.

Sources & evidence

ORD record: ord-db25d47d1d494e09af4fbc7d88bbbe0f
Source dataset: uspto-grants-2003_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06576797B1

Reaction notes

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