Nitric Acid → HCID 178512435, compound

HRID 1370070Notes

Reaction equation

HRID 1370070 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][N:6]=[CH:5]2.[N:11]#[C:12][NH2:13].[N+:14]([O-:17])([OH:16])=[O:15]>>[N+:14]([O-:17])([O-:16])=[O:15].[NH:7]1[C:8]2[C:4](=[CH:3][C:2]([NH:1][C:12]([NH2:13])=[NH2+:11])=[CH:10][CH:9]=2)[CH:5]=[N:6]1

Participants

4

Reactant 3

HCID 944Nitric AcidHCID 9864CyanamideHCID 880121H-Indazol-5-amine

Product 1

HCID 178512435HCID 178512435, compound

Procedure

Indazol-5-ylguanidinium nitrate was prepared from 5-aminoindazole (4.0 g, mmol), cyanamide (1.89 g, 45.1 mmol) and concentrated HNO3 (2.8 ml) to give the desired material as a solid m.p. 252-254°.

Sources & evidence

ORD record
ord-eeef5f3c8ffc40b4aaaa3620ffb656bb
Source dataset
uspto-grants-2003_06
Patent number
US06579983B1

Reaction notes

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