HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-(trifluoromethyl)benzenesulfonyl chloride → HCID 18511633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-(trifluoromethyl)benzenesulfonyl chloride | HCID 2736675 | — |
| Reactant | HCID 18511540 | HCID 18511540 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18511633 | HCID 18511633 | — |
Reaction Steps
2-Chloro-N-(3,5-dichloro-4-isoquinolin-3-ylmethyl-phenyl)-4-trifluoromethyl-benzenesulfonamide was synthesized (65%) from 3,5-dichloro-4-isoquinolin-3-ylmethyl-phenylamine (236), 2-chloro-4-trifluromethylbenzenesulfonyl chloride (Maybridge) and pyridine (EM) in a similar manner as described in Examples 70-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583157B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-7c6132bb4bcf4818894aeacabb4fb7fd |
| Source note | uspto-grants-2003_06 |