2,6-Dichlorobenzothiazole → 3,5-Dichloro-4-(6-chloro-benzothiazol-2-yloxy)-phenylamine

HRID 1370520Notes

Reaction equation

HRID 1370520 reaction equation
Cl[C:2]1[S:3][C:4]2[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:5]=2[N:6]=1.[NH2:12][C:13]1[CH:18]=[C:17]([Cl:19])[C:16]([OH:20])=[C:15]([Cl:21])[CH:14]=1>>[Cl:19][C:17]1[CH:18]=[C:13]([NH2:12])[CH:14]=[C:15]([Cl:21])[C:16]=1[O:20][C:2]1[S:3][C:4]2[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:5]=2[N:6]=1

Participants

3

Reactant 2

HCID 771762,6-DichlorobenzothiazoleHCID 800374-Amino-2,6-dichlorophenol

Product 1

HCID 221487763,5-Dichloro-4-(6-chloro-benzothiazol-2-yloxy)-phenylamine

Procedure

3,5-Dichloro-4-(6-chloro-benzothiazol-2-yloxy)-phenylamine was synthesized (65%) from 2,6-dichlorobenzotiazole (259) and 4-amino-2,6-dichlorophenol (Aldrich) in a similar manner as described in Example 417.

Sources & evidence

ORD record
ord-354e248e1fbf43c69a45240500fceb7d
Source dataset
uspto-grants-2003_06
Patent number
US06583157B2

Reaction notes

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