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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1370556Generated: October 30, 2026

Water → HCID 21685517, compound

https://huagongshe.com/reaction/1370556

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantBenzhydrylamineHCID 7036—
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
SolventDichloromethaneHCID 6344—
ProductHCID 21685517HCID 21685517—

Reaction Steps

Benzhydrylamine (1.83 g) was dissolved in dichloromethane (3.0 ml). Carbonyldiimidazole (1.78 g) was added to the solution. The mixture was stirred at room temperature overnight. Water and dichloromethane were added thereto. The mixture was stirred, and then extracted with dichloromethane. The organic layer was dried over anhydrous magnesium sulfate. The solvent was then removed by distillation is to give imidazole-1-carboxylic acid benzhydrylamide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06583144B2
Source datasetuspto-grants-2003_06
ORD IDord-3bd32c1dd9bc48078a388af86d101e2b
Source noteuspto-grants-2003_06