HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21685517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzhydrylamine | HCID 7036 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21685517 | HCID 21685517 | — |
Reaction Steps
Benzhydrylamine (1.83 g) was dissolved in dichloromethane (3.0 ml). Carbonyldiimidazole (1.78 g) was added to the solution. The mixture was stirred at room temperature overnight. Water and dichloromethane were added thereto. The mixture was stirred, and then extracted with dichloromethane. The organic layer was dried over anhydrous magnesium sulfate. The solvent was then removed by distillation is to give imidazole-1-carboxylic acid benzhydrylamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583144B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-3bd32c1dd9bc48078a388af86d101e2b |
| Source note | uspto-grants-2003_06 |