HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromonaphthalene → 9-(Naphthalen-1-yl)anthracene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromonaphthalene | HCID 7001 | — |
| Reactant | Anthrone | HCID 7018 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 9-(Naphthalen-1-yl)anthracene | HCID 18510032 | — |
Reaction Steps
A Grignard reagent was prepared from 1-bromonaphthalene and magnesium in diethyl ether under an inert atmosphere. The reagent was reacted with 9-anthrone. The reaction was quenched with hydrochloric acid, and the mixture was purified as usual, to give the desired 9-α-naphthylanthracene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06582837B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-2c7839d733b142d0881695e96db12e4f |
| Source note | uspto-grants-2003_06 |