Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | 1,3-Cyclohexadiene | HCID 11605 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86587025 | HCID 86587025 | — |
Reaction Steps
To a solution of maleic anhydride (10.30 g) in toluene (100 ml) was added 1,3-cyclohexadiene (8.41 g). The mixture was refluxed for 3 hours. After cooling to 25° C., the solvent was evaporated at reduced pressure. The solid was recrystallized from EtOAC/hexane to yield bicyclo[2.2.2]oct-en-2,3-dicarboxylic anhydride as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06583206B2 |
|---|
| Source dataset | uspto-grants-2003_06 |
|---|
| ORD ID | ord-d734b38838e84b99bc03bb845db5f2a7 |
|---|
| Source note | uspto-grants-2003_06 |
|---|
