Methyl Ethyl Ketone → 4'-Methanesulfonyl-3,4-dipropyloxy-biphenyl

Participants

Reaction Conditions

Reaction Steps

4′-methanesulfonyl-biphenyl-3,4-diol (30 mg) and potassium carbonate (38 mg) were dissolved in methylethylketone. Afterward, propane iodide (0.032 ml) was added and refluxed for 3 hours at 100° C. After filtering just potassium carbonate, the residue was separated through a silica gel attributed chromatography (an eluting agent: ethylacetate/n-hexane=1/1, v/v). As a result, the present compound (30 mg, productive yield 90%) was obtained.

Provenance & Evidence