HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 73195160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 11240434 | HCID 11240434 | — |
| Reactant | HCID 69959678 | HCID 69959678 | — |
| Solvent | Water methylene chloride | HCID 21908982 | — |
| Product | HCID 73195160 | HCID 73195160 | — |
Reaction Steps
The acid chloride obtained starting from 6.5 g (28.5 mmol) of the acid obtained in Step E and 5 ml of oxalyl chloride are added dropwise to a suspension of N,O-dimethylhydroxylamine chloride (5.6 g) in a mixture of CH2Cl2/H2O in the presence of 3 g of Na2CO3. The protected acid is obtained in the form of a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583319B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-a41a01fd2fdd4aa58f30d0d92d765f0f |
| Source note | uspto-grants-2003_06 |