Piperonal → N-(1,3-benzodioxol-5-ylmethyl)-N-(2-methyl-3-nitrophenyl)amine

HRID 1370790Notes

Reaction equation

HRID 1370790 reaction equation
[CH3:1][C:2]1[C:8]([N+:9]([O-:11])=[O:10])=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].[O:12]1[C:16]2[CH:17]=[CH:18][C:19]([CH:21]=O)=[CH:20][C:15]=2[O:14][CH2:13]1>>[O:12]1[C:16]2[CH:17]=[CH:18][C:19]([CH2:21][NH:4][C:3]3[CH:5]=[CH:6][CH:7]=[C:8]([N+:9]([O-:11])=[O:10])[C:2]=3[CH3:1])=[CH:20][C:15]=2[O:14][CH2:13]1

Participants

3

Reactant 2

HCID 8438PiperonalHCID 117832-Methyl-3-nitroaniline

Product 1

HCID 18512119N-(1,3-benzodioxol-5-ylmethyl)-N-(2-methyl-3-nitrophenyl)amine

Procedure

2-Methyl-3-nitroaniline and 1,3-benzodioxole-5-carbaldehyde were processed as described in Example 1C to provide the title compound.

Sources & evidence

ORD record
ord-928ba5abbbbb40dc921e05f8f2b329f5
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

Loading…