2-Methyl-3-nitroaniline → N-(4-{[(2Z)-3-bromoprop-2-enyl]oxy}benzyl)-N-(2-methyl-3-nitrophenyl)amine

HRID 1370825Notes

Reaction equation

HRID 1370825 reaction equation
[Br:1]/[CH:2]=[CH:3]\[CH2:4][O:5][C:6]1[CH:13]=[CH:12][C:9]([CH:10]=O)=[CH:8][CH:7]=1.[CH3:14][C:15]1[C:21]([N+:22]([O-:24])=[O:23])=[CH:20][CH:19]=[CH:18][C:16]=1[NH2:17]>>[Br:1]/[CH:2]=[CH:3]\[CH2:4][O:5][C:6]1[CH:13]=[CH:12][C:9]([CH2:10][NH:17][C:16]2[CH:18]=[CH:19][CH:20]=[C:21]([N+:22]([O-:24])=[O:23])[C:15]=2[CH3:14])=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 117832-Methyl-3-nitroanilineHCID 865862254-{[(2Z)-3-bromoprop-2-enyl]oxy}benzaldehyde

Product 1

HCID 86586226N-(4-{[(2Z)-3-bromoprop-2-enyl]oxy}benzyl)-N-(2-methyl-3-nitrophenyl)amine

Procedure

The product from Example 57A and 2-methyl-3-nitroaniline were processed as described in Example 6A to provide the title compound.

Sources & evidence

ORD record
ord-662f35954957447e8e9f9f4b1a1dc436
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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