(3-Bromophenyl)boronic acid → HCID 18511966, compound

HRID 1370843Notes

Reaction equation

HRID 1370843 reaction equation
[CH2:1]([N:8]([CH2:19][C:20]1[CH:25]=[CH:24][C:23]([OH:26])=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Br:27][C:28]1[CH:29]=[C:30](B(O)O)[CH:31]=[CH:32][CH:33]=1>>[CH2:1]([N:8]([CH2:19][C:20]1[CH:25]=[CH:24][C:23]([O:26][C:32]2[CH:31]=[CH:30][CH:29]=[C:28]([Br:27])[CH:33]=2)=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 2734318(3-Bromophenyl)boronic acidHCID 18512152HCID 18512152, compound

Product 1

HCID 18511966HCID 18511966, compound

Procedure

The product from Example 65B and 3-bromophenylboronic acid were processed as described in Example 48A to provide the title compound. MS (ESI+) m/z 504 (M+H)+.

Sources & evidence

ORD record
ord-9afd99ab430a4ab5a743df612c683ace
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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