3-[(Tert-butyldimethylsilyl)oxy]propan-1-ol → HCID 68859815, compound

HRID 1370852Notes

Reaction equation

HRID 1370852 reaction equation
[CH2:1]([N:8]([CH2:19][C:20]1[CH:33]=[CH:32][C:23]([O:24][C:25]2[CH:26]=[C:27]([OH:31])[CH:28]=[CH:29][CH:30]=2)=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Si:34]([O:41][CH2:42][CH2:43][CH2:44]O)([C:37]([CH3:40])([CH3:39])[CH3:38])([CH3:36])[CH3:35]>>[CH2:1]([N:8]([CH2:19][C:20]1[CH:33]=[CH:32][C:23]([O:24][C:25]2[CH:30]=[CH:29][CH:28]=[C:27]([O:31][CH2:44][CH2:43][CH2:42][O:41][Si:34]([C:37]([CH3:38])([CH3:40])[CH3:39])([CH3:35])[CH3:36])[CH:26]=2)=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 40777913-[(Tert-butyldimethylsilyl)oxy]propan-1-olHCID 185122603-(4-{[Benzyl(2-methyl-3-nitrophenyl)amino]methyl}phenoxy)phenol

Product 1

HCID 68859815HCID 68859815, compound

Procedure

The product from Example 61F and 1-t-butyldimethylsilyloxypropan-3-ol were processed as in Example 61G to provide the title compound.

Sources & evidence

ORD record
ord-c496944c753f4eb3836a1b699229392e
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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