HCID 18512201, compound → HCID 18512206, compound

Participants

Reaction Steps

The product from Example 87D (0.045 g, 0.0784 mmoles) in 1:1 ethyl acetate/TBF (4 mL) was added to a degassed flask charged with 10% palladium on carbon catalyst (0.050 g). Reaction mixture was degassed again and stirred vigorously at room temperature under an atmosphere of hydrogen for one hour. The reaction mixture was filtered through a pad of celite, and filtrate concentrated under reduced pressure to provide the title compound with no further purification (0.035 g, 82%). MS (ESI+) m/z 547 (M+H)+.

Provenance & Evidence