Methanamine, N-methoxy-, hydrochloride (1:1) → HCID 18511970, compound

HRID 1370871Notes

Reaction equation

HRID 1370871 reaction equation
[CH2:1]([N:8]([CH2:21][C:22]1[CH:30]=[CH:29][C:25]([C:26](O)=[O:27])=[CH:24][CH:23]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][S:16]([CH3:19])(=[O:18])=[O:17])[C:10]=1[CH3:20])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl.[CH3:32][NH:33][O:34][CH3:35]>>[CH2:1]([N:8]([CH2:21][C:22]1[CH:30]=[CH:29][C:25]([C:26]([N:33]([O:34][CH3:35])[CH3:32])=[O:27])=[CH:24][CH:23]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][S:16]([CH3:19])(=[O:17])=[O:18])[C:10]=1[CH3:20])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 81138Methanamine, N-methoxy-, hydrochloride (1:1)HCID 18512178HCID 18512178, compound

Product 1

HCID 18511970HCID 18511970, compound

Procedure

The product from Example 88A and N,O-dimethylhydroxylamine hydrochloride were processed as described in Example 68D to provide the title compound. MS (ESI+) m/z 468 (M+H)+.

Sources & evidence

ORD record
ord-23576c4be9894529b97725e0d027877a
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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