2-Methyl-3-nitroaniline → N-{4-[3-(allyloxy)-5-methoxyphenoxy]benzyl}-N-(2-methyl-3-nitrophenyl)amine

HRID 1370881Notes

Reaction equation

HRID 1370881 reaction equation
[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[C:18]([O:20][CH3:21])[CH:19]=1)[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][CH:10]=1)[CH:2]=[CH2:3].[CH3:22][C:23]1[C:29]([N+:30]([O-:32])=[O:31])=[CH:28][CH:27]=[CH:26][C:24]=1[NH2:25]>>[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[C:18]([O:20][CH3:21])[CH:19]=1)[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][NH:25][C:24]2[CH:26]=[CH:27][CH:28]=[C:29]([N+:30]([O-:32])=[O:31])[C:23]=2[CH3:22])=[CH:11][CH:10]=1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 117832-Methyl-3-nitroanilineHCID 185123734-[3-(Allyloxy)-5-methoxyphenoxy]benzaldehyde

Product 1

HCID 18512102N-{4-[3-(allyloxy)-5-methoxyphenoxy]benzyl}-N-(2-methyl-3-nitrophenyl)amine

Procedure

The product from Example 90B and 2-methyl-3-nitroaniline were processed as in Example 6A to provide the title compound. MS (ESI−) m/z 419 (M−H)−.

Sources & evidence

ORD record
ord-441fadc684f14bd7af996ec8d496ea9d
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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