4-Amino-1-butanol → HCID 18512157, compound

Participants

Reaction Steps

The product from Example 104A and 4-amino-1-butanol were processed as described in Example 147 to provide the title compound. 1H NMR (500 MHz, DMSO-d6) δ8.95 (s, 1 H), 7.74 (t, 1 H), 7.26 (m, 6 H), 7.19 (m, 3 H), 7.04 (t, 1 H), 6.96 (m, 2 H), 6.86 (m, 4 H), 4.03 (d, 4 H), 3.35 (m, 2 H), 3.03 (m, 2 H), 2.91 (s, 3 H), 2.78 (t, 2 H), 2.39 (s, 3 H), 2.34 (m, 2 H), 1.37 (m, 4 H); MS (ESI+) m/z 616 (M+H)+.

Provenance & Evidence