H-Gln-OtBu hydrochloride → HCID 21130132, compound

Participants

Reaction Steps

The product from Example 233 and L-glutamine tert-butyl ester hydrochloride were processed as described in Example 251A and 258B to provide the titled compound. 1H NMR (500 MHz, DMSO-d6) δ12.00-12.89 (br.s, 1 H), 8.94 (s, 1 H), 8.13 (d, 1 H), 7.24 (m, 8 H), 6.98 (m, 7 H), 6.82 (d, 2 H), 6.73 (s, 1 H), 4.16 (m, 1 H), 4.05 (s, 2 H), 4.00 (s, 2 H), 3.95 (m, 2 H), 2.91 (s, 3 H), 2.39 (s, 3 H), 2.29 (t, 2 H), 2.12 (m, 2 H), 1.94 (m, 3 H), 1.74 (m, 1 H), MS (ESI+) m/z 703 (M+H)+.

Provenance & Evidence