2-Methyl-3-nitroaniline → HCID 11350329, compound

HRID 1370970Notes

Reaction equation

HRID 1370970 reaction equation
[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[CH:18][C:19]=1[F:20])[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][CH:10]=1)[CH:2]=[CH2:3].[CH3:21][C:22]1[C:28]([N+:29]([O-:31])=[O:30])=[CH:27][CH:26]=[CH:25][C:23]=1[NH2:24]>>[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[CH:18][C:19]=1[F:20])[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][NH:24][C:23]2[CH:25]=[CH:26][CH:27]=[C:28]([N+:29]([O-:31])=[O:30])[C:22]=2[CH3:21])=[CH:11][CH:10]=1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 117832-Methyl-3-nitroanilineHCID 11403025HCID 11403025, compound

Product 1

HCID 11350329HCID 11350329, compound

Procedure

The product from Example 305D and 2-methyl-3-nitroaniline were processed as in Example 6A to provide the title compound. MS (ESI−) m/z 407 (M−H)+.

Sources & evidence

ORD record
ord-f48f6e06c9084159ba3c9c08ac94364d
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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