HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[(2R)-4-(3,4-Dichlorobenzyl)morpholin-2-yl]methanamine → 4-Nitrophenyl [(2R)-4-(3,4-dichlorobenzyl)morpholin-2-yl]methylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[(2R)-4-(3,4-Dichlorobenzyl)morpholin-2-yl]methanamine | HCID 11346392 | — |
| Reactant | 4-Nitrophenyl [4-(3,4-dichlorobenzyl)morpholin-2-yl]methylcarbamate | HCID 11539448 | — |
| Product | 4-Nitrophenyl [(2R)-4-(3,4-dichlorobenzyl)morpholin-2-yl]methylcarbamate | HCID 86760342 | — |
Reaction Steps
Intermediate 14 was prepared in an analogous manner to Intermediate 10 from Intermediate 12 (0.21 g) and 4-nitrophenylchloroformate (0.17 g) to yield the title compound (0.23 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-443e9b48fac345d8b3297cd54b99b9ae |
| Source note | uspto-grants-2007_01 |