HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatobenzonitrile → HCID 10223803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatobenzonitrile | HCID 2733315 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | HCID 10223803 | HCID 10223803 | 67.5% |
Reaction Steps
Example 5 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 3-isocyanatobenzonitrile (0.0196 g) to give the title compound (0.0257 g). LC-MS (System A): Rt 2.29 mins, Mass Spectrum m/z 419 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-dade016c71ed4a43854bc555e0c9bee4 |
| Source note | uspto-grants-2007_01 |