HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl isocyanate → N-Allyl-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl isocyanate | HCID 15123 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | N-Allyl-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea | HCID 10109024 | — |
Reaction Steps
Example 10 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 3-isocyanatoprop-1-ene (12.0 μl) to give the title compound (0.027 g). LC-MS (System A): Rt 1.93 mins, Mass Spectrum m/z 358 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-0f1d35f9db0e4cb6b2c2188a58fd3772 |
| Source note | uspto-grants-2007_01 |