HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Naphthyl isocyanate → N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}-N'-(1-naphthyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Naphthyl isocyanate | HCID 66589 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}-N'-(1-naphthyl)urea | HCID 10160685 | — |
Reaction Steps
Example 31 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 1-isocyanatonaphthalene (19.6 μl) to give the title compound (0.0304 g). LC-MS (System A): Rt 2.43 mins, Mass Spectrum m/z 444 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-531a09b145644e41893d76345726d72a |
| Source note | uspto-grants-2007_01 |