HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1371555Generated: November 1, 2026
1-Methylpiperazine → HCID 21071294, compound
https://huagongshe.com/reaction/1371555
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 22170839 | HCID 22170839 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21071294 | HCID 21071294 | — |
Reaction Steps
A mixture of 3-(3-chloro-propoxy)-phenylacetic acid (0.5 g, 2.2 mmol) and N-methylpiperazine (1.9 mL) was heated at 60° C. overnight. The reaction was diluted with water and purified by preparative HPLC to give the product as a clear gel. (0.6 g, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07157476B2 |
|---|
| Source dataset | uspto-grants-2007_01 |
|---|
| ORD ID | ord-865f1d3b290a4c6d8fdfd4e3e66e21e7 |
|---|
| Source note | uspto-grants-2007_01 |
|---|
