HCID 58778279, compound → HCID 58778267, compound

Participants

Reaction Steps

Tert-butyl 2-(2-methoxyphenylamino)-1-phenylethylcarbamate (0.54 g, 1.6 mmol) was dissolved in 10 mL 4N HCl in dioxane. After one hour the reaction mixture was concentrated to dryness, taken up in ethyl acetate, and the organic layer washed with 1N NaOH and then dried over sodium sulfate and concentrated to give the free amine as a brown oil, 0.35 g, 1.45 mmol, 90% yield.

Provenance & Evidence