HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrodibenzofuran → 3-Dibenzofuranamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrodibenzofuran | HCID 72897 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Dibenzofuranamine | HCID 20061 | — |
Reaction Steps
Combine 3-nitrodibenzofuran (22.0 g, 0.1 mol) and Raney nickel (2.75 g), and ethanol (365 ml) and hydrogenate at room temperature and 40 psi (276 kPa). After 18 hours, filter and concentrate the filtrate to residue. Chromatograph the residue eluting with 9:1 hexane:EtOAc to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157488B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-9738013b52af4902825d241884ee1d3d |
| Source note | uspto-grants-2007_01 |