L-Tartaric acid → HCID 86602622, compound

Participants

Reaction Steps

Add L-(+)-tartaric acid (295 mg, 1.96 mmol) in methanol to a solution of N-(2-(7-fluoro-1H-indol-3-yl)ethyl)-3-(2,2,2-trifluoroethoxy)benzylamine (720 mg, 1.96 mmol) in ethyl acetate. Concentrate under reduced pressure the resulting solution to give a clear colorless oil. Crystallize the oil from diethyl ether to give the title compound: mp 118–119° C. MS(m/e): 367 (M+1), 365. (M−1). Calculated for C19H18F4N2O.C4H6O6: Calcd: C, 53.49; H 4.68; N, 5.42. Found: C, 53.21; H, 4.55; N, 5.41.

Provenance & Evidence