HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclen tetrahydrochloride → 1,4,7,10-Tetraazacyclododecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclen tetrahydrochloride | HCID 11652630 | — |
| Reactant | Cucurbit[8]uril | HCID 16133299 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1,4,7,10-Tetraazacyclododecane | HCID 64963 | — |
Reaction Steps
120.0 mg of cyclen tetrahydrochloride (1,4,7,10-tetraazacyclodecane tetrahydrochloride) and 100.0 mg of cucurbit[8]uril were dissolved in water. Heating followed by slow cooling of the solution produced an inclusion complex in which a cyclen molecule was encapsulated in the cavity of cucurbit[8]uril as a colorless crystalline material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160466B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-b6b8935b53c644f8ac3ea17e26985234 |
| Source note | uspto-grants-2007_01 |