HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1'-Biphenyl, 4-(bromomethyl)- → 3-benzyl-6-(biphenyl-4-ylmethylsulfanyl)-5-methyl-1H-pyrimidine-2,4-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1'-Biphenyl, 4-(bromomethyl)- | HCID 257716 | — |
| Edukt | 3-Benzyl-6-mercapto-5-methyl-1H-pyrimidine-2,4-dione | HCID 21074061 | — |
| Produkt | 3-benzyl-6-(biphenyl-4-ylmethylsulfanyl)-5-methyl-1H-pyrimidine-2,4-dione | HCID 21073997 | — |
Reaktionsschritte
The product of Example 2, Step (C) was treated with 4-phenylbenzyl bromide as in Example 2, Step (D) to give 3-benzyl-6-(biphenyl-4-ylmethylsulfanyl)-5-methyl-1H-pyrimidine-2,4-dione. MS (APCI), m/z ([M+H]+) 415.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07160893B2 |
| Quelldatensatz | uspto-grants-2007_01 |
| ORD ID | ord-8a022b6bd5b34593bb682e97f09e4443 |
| Quellennotiz | uspto-grants-2007_01 |