HCID 18005695, compound → HCID 18005677, compound

HRID 1373123Notes

Reaction equation

HRID 1373123 reaction equation
[CH3:1][N:2]([CH3:19])[CH2:3][CH2:4][N:5]([C:10]1[CH:11]=[C:12]([N+:16]([O-])=O)[CH:13]=[CH:14][CH:15]=1)[S:6]([CH3:9])(=[O:8])=[O:7]>[Pd]>[CH3:1][N:2]([CH3:19])[CH2:3][CH2:4][N:5]([C:10]1[CH:11]=[C:12]([CH:13]=[CH:14][CH:15]=1)[NH2:16])[S:6]([CH3:9])(=[O:8])=[O:7]

Participants

3

Reactant 1

HCID 18005695HCID 18005695, compound

Product 1

HCID 18005677HCID 18005677, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Prepared analogously to Example 1d by catalytic hydrogenation of 1.9 g (6.8 mmol) of 3-[N-(2-dimethylamino-ethyl)-N-methylsulphonyl-amino]-nitrobenzene over palladium/charcoal.

Sources & evidence

ORD record
ord-ae5ca109a11a42cc9bfbeaa62319b999
Source dataset
uspto-grants-2007_01
Patent number
US07160901B2

Reaction notes

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