HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21361363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 2,6-Diethyl-2,3,6-trimethyl-1-(1-phenylethoxy)piperidin-4-ol | HCID 22341851 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21361363 | HCID 21361363 | 870.1% |
Reaction Steps
In analogy to example 1 were reacted 6.36 g (2 mmol) of 2,6-diethyl-2,3,6-trimethyl-1-(1-phenyl-ethoxy)-piperidin-4-ol with 1.81 g (2 mmol) of acryloyl chloride and 2.02 g (2 mmol) of triethylamine in toluene to give 6.5 g (87%) acrylic acid 2,6-di-ethyl-2,3,6-trimethyl-1-(1-phenyl-ethoxy)-piperidin-4-yl ester as yellowish liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160966B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-82e9be55d9c94af8a7566e9b6ba7d0c1 |
| Source note | uspto-grants-2007_01 |