HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 4'-Hydrazino-2,2':6',2''-terpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 4'-Chloro-2,2':6',2''-terpyridine | HCID 667748 | — |
| Solvent | (+-)-2-Butanol | HCID 6568 | — |
| Product | 4'-Hydrazino-2,2':6',2''-terpyridine | HCID 10539488 | — |
Reaction Steps
4 ml (126 mmol) of hydrazine are added to 600 mg (2.2 mmol) of 4′-chloro-[2,2′;6′,2″]-terpyridine in 12 ml of 2-butanol. The mixture is heated at reflux for 17 hours and cooled, and [2,2′;6′,2″]terpyridin-4′-yl-hydrazine is filtered off in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07161005B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-8f26a72bb9c44fd3b9a732bd32cb2f68 |
| Source note | uspto-grants-2007_01 |