Thionyl Chloride → HCID 87820185, compound

HRID 1373478Notes

Reaction equation

[C:1]([NH:4][CH2:5][CH2:6][C:7]1[C:11]2[CH:12]=[C:13]([C:16]([OH:18])=O)[CH:14]=[CH:15][C:10]=2[O:9][CH:8]=1)(=[O:3])[CH3:2].S(Cl)([Cl:21])=O>>[C:1]([NH:4][CH2:5][CH2:6][C:7]1[C:11]2[CH:12]=[C:13]([C:16]([Cl:21])=[O:18])[CH:14]=[CH:15][C:10]=2[O:9][CH:8]=1)(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 69410961HCID 69410961, compound

Product 1

HCID 87820185HCID 87820185, compound

Procedure

5 mmol of the product obtained in Step E are dissolved in 40 ml of thionyl chloride. After stirring under an inert atmosphere for 1 hour, the thionyl chloride is removed by evaporation under reduced pressure to yield the title product.

Workup

customthe thionyl chloride is removed by evaporation under reduced pressure

Sources & evidence

ORD record: ord-7782a26d7f9f4d938166ccb263314f13
Source dataset: uspto-grants-2007_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07161035B2

Reaction notes

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