HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl (4R)-4-{[(benzyloxy)carbonyl]amino}pentanoate → HCID 58781983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl (4R)-4-{[(benzyloxy)carbonyl]amino}pentanoate | HCID 11109586 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58781983 | HCID 58781983 | 106.3% |
Reaction Steps
To a solution of tert-butyl (4R)-4-{[(benzyloxy)carbonyl]amino}pentanoate (3.5 g, 11.4 mmol) in methanol (35 ml) was added Pd—C (0.7 g) and the mixture was stirred under a hydrogen atomosphere for 3 hours. Catalyst was-removed by filtration and the solvent was removed in vacuo to give tert-butyl(4R)-4-aminopentanoate (2.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07163936B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-62a1634cec9145a4826dd171d59b7ea3 |
| Source note | uspto-grants-2007_01 |